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To simultaneously quantify the levels of persulfide and polysulfide sulfur, one aliquot of reaction mixture (100 Β΅L) was blocked with IAM-TPP (250 Β΅M) for procedure A and another aliquot of the same reaction (100 Β΅L) was blocked with IAM (250 Β΅M) for procedure B for 20 min at RT, protected from light
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